Pre – Flashed Paper Negatives for Pinhole Photography

To achieve a paper negative with a wide contrast range it is helpful to pre-flash or expose the paper very briefly to white light in the darkroom before exposing in your pinhole camera. This pre-flash will reduce the contrast of your negative and also decrease the exposure time. Pre-flashing slightly increases the exposure in the shadow detail areas without affecting the highlight detail.

Each brand of paper will require its own pre-flash exposure. Use the following steps to determine the correct exposure for your brand of paper.

  1. Set enlarger to F16 and insert a # 3 filter. Set the head to the highest position at the top of the column.  Alternatively you can use a dim light bulb suspended 3 feet or more above your paper. Try a 7-watt bulb for this.
  2. Make a test strip with 5 sets of 1-second exposures.
  3. The correct pre-flash is the exposure for the first strip that is barely visible. If your test sheet is all white increase the exposure per strip, if it is too dark, decrease the exposure for each strip.
  4. Write down the enlarger station, head height, f-stop and exposure used in your notes for further reference.
  5. Expose all the sheets you will be using and keep them separated from your un-flashed paper. I put mine in the bottom of the black bag under a piece of matte board.

Digital or traditional negatives

Most hand-applied emulsions require such a great amount of exposure that direct enlarger projection onto them is not possible. Contact printing is required under a strong UV light source. With contact printing you need a negative the same size as your print. These can be shot in a large format camera, in the darkroom with special litho films or through a computer and inkjet printer.


Making traditional negatives for contact printing

Most hand-applied emulsions require such a great amount of exposure that direct enlarger projection onto them is not possible. Contact printing is required under a strong UV light source. A few  options are available to the traditional photographer wishing to work in the darkroom instead of the computer to make contact size negatives, film shot in camera, litho film shot in a pinhole camera or litho film printed in the darkroom.

Traditional film shot in camera: Processed film from traditional cameras can be used but your print size is limited to your camera format. Many practitioners use large format cameras for this reason. For a full tonal range in the print, the negative should have a long density range of at least 1.8, extending from base+fog at around 0.2 to a Dmax of 2 or more. This is achieved by “overdeveloping” the negative to the extent of 70%-80% more development.

Litho film shot in a pinhole camera: Standard continuous tone panchromatic film is expensive in large sizes, and must be handled and processed in complete darkness because of its sensitivity to all colors of light. Therefore, it’s usually more practical to use “litho or ortho film” (orthochromatic–not sensitive to red light), which is much less expensive, available in many sizes and can be processed for continuous tonality or high contrast under red safelight. Litho films were designed to record extreme contrast for the printing industry. Artists have discovered they can obtain continuous tone by developing in dilute paper developers or making their own developers to control the films contrast. With litho film you can make your own pinhole camera and shoot original negatives to the size of your final print.

Litho film printed in the darkroom: Below are four methods of making contact sized litho films in the darkroom. Each of the following methods varies somewhat in the complexity of the operation and the degree of tonal information it yields.

1) Enlargement of original negative to full-size ortho positive, contact printing of full-size positive to make full-size negative: This is expensive because you are using full-size film for both generations.

Exposure: Choose your original negative, keeping in mind that any lack of detail in the original will be amplified in the following generations of litho’s. Test strip onto the emulsion side of the litho film. The emulsion side looks lighter then the base under red safelight. Process the film and inspect it in regular room light.

Be careful not to scratch the soft litho emulsion during processing. Therefore, carry out all processing emulsion side up.

Develop with constant agitation for 5 minutes in diluted paper developer (dilute 2-3 times more then you would normally for paper development). The developer will exhaust quickly so replenish or change often.
Stop for 30 seconds.
Fix for 1 minute.
Use fixer remover to speed up wash time.
Tray wash with frequent agitation for 5-10 minutes.
Treat with a wetting agent.
Hang to dry by one corner in the drying cabinet.

When enlarging try to maintain the most even tonal range as possible with good detail retention in all areas. This will prevent too great a loss of detail when contacting to the negative stage.

When you have determined the best exposure, make the full exposure for the positive litho. Treat litho film essentially as you would normal printing paper, and do all dodging, burning, and other manipulations as well. All errors will be amplified in future generational processing.

Contacting from the positive to the full-size negative should be done so that the emulsion sides of both pieces of film are in contact; this gives the sharpest information transfer. Make sure that the glass you use to hold down the film is clean and heavy enough to cause tight, flat contact. For the most control, contact expose with a light source such as enlarger light through a small lens aperture; this allow for best detail retention. Remember also that dodging and burning can also be done during contact printing if necessary.

Notes:

A) Large sheets of film attract dust rather well, and care must be taken to keep the film surface clean before and during exposure.

B) The litho density required for contact printing onto each of the various hand applied emulsions varies slightly, and you will need to go all the way through a process to find out exactly what is required. Generally though, gum printing requires lithos of slightly greater contrast, and cyanotype or Van Dykes need flatter lithos.

2) Enlargement of original negative onto 4 x 5 ortho film then enlargement of 4 x 5 positive onto full-size litho film: Ilford and other manufacturers make a continuous tone orthochromatic film in 4×5 inch size that has many advantages: the tonal capacity is much better than that of litho film (even when developed for continuous tonality) and thus less detail is lost when enlarging from the ortho positive to the litho negative, and it is much easier to dodge and burn during that enlargement than it is during contact printing.

Exposure: Test strip and expose from the original negative onto the 4 x 5 ortho according to the information indicated in the previous section. Again try for as extended and flat a tonal range as possible.

Processing: Ortho film should be handled as carefully as indicated for litho processing. The only difference in processing instructions should be in the development: Tray develop in stock film developer with constant agitation for 6 minutes. Cover the developer tray with an opaque cover to minimize exposure to the safelight. Expose and process the full-size litho negative as outlined earlier.

3) Copying negative using a slide copier: Another possibility is to copy your original negatives in a slide copying system using negative film. This results in a roll film positive which can then be directly enlarged to the full-size negative litho film, while still preserving the original negative for standard enlargement.

4) Paper positive, contact printed to paper negative: A great financial savings can be made at the expense of quality (or to achieve a personal quality) by substituting printing paper for litho film in method #1. If you decide to make paper rather than film transparencies, be sure to use the thinnest paper possible otherwise your printing times onto hand applied emulsions will be very long. Do not use paper with the manufacturers’ name stamped on the back unless you want it to appear in your print. Processing and exposure of paper negatives should be for slightly a contrasty tonality to account for the density of the paper. The paper negative can be made more transparent by applying a thin coating of hot melted paraffin or a thin coat of oil to the back of the paper. One good thing about making paper negatives is that you have very good control over the tonality and image quality.


Making Digital Negatives with Chart Throb

This instructions includes complete information for calibrating your system from the inkjet printer to the final print. For use at UMBC you can skip section I and go right to section II.

Section I
Finding the correct settings for your negative:

Before making your negative, you need to find the correct exposure time and color for the process. Exposure times can change with different papers and application methods so try to standardize these as much as possible.

  • Coat your paper your normal way and dry it. Make a test strip using a clear sheet of your transparency film. Process following your standard procedures. What you are looking for is the exposure that represents the minimum time it takes to make maximum density.
  • Once you find the correct time, coat another piece of paper, dry, and print with the positive transparency of the HSB-Array (multicolor RGB chart) located at http://www.inkjetnegative.com/images/RNP/HSLArrayAdobe98.tif

Why this is important: Not all inkjet printers can lay down enough density to produce decent negatives for some long tonal range processes (salted paper, new cyanotype, palladium…). This is why we make colorized negatives, to find an ink color, which acts as a color filter, blocking more UV-light than gray-tone negatives can do. When printing a negative with this particular color we can use its UV blocking density to produce a better tonal range in our final print.

What we are looking for on this chart: Please note that this chart will be a monotone grayscale depending on which process you are using. What we are trying to find is a nice tonal range (bright whites and dark blacks) for the negative. Choose a column that presents a smooth grayscale and choose your point based on that.

  • In Photoshop, open the digital file of the RNP/HSB-Array chart. Locate the same point that you have just chosen for your negative. Using the eyedropper tool, click on that point on the color chart. In the info dialog box on the right of the screen, you will see an RGB color reading for that point. Make note of the numbers!

What to do with the color information: Now that we know what color will give us the best tonal range, we need to print a Chart Throb. Chart Throb is an javascript that works in Photoshop Scripts . You can download it from http://www.botzilla.com/blog/archives/000544.html. To access Chart Throb at UMBC go to File/Scripts/ChartThrob.jsx in Photoshop.

  • In Photoshop, open the Grayscale Chart Throb.
  • Invert your image: Image/Adjustments/Invert
  • In your layers palate, click on the “Create New Fill or Adjustment Layer” button (it looks like a half white/black circle), and choose “solid color.” In the R, G, and B boxes, enter the numbers that you just made note of from the RNP/HSB-Array chart. Click OK.

  • Under the blending mode drop down menu in your layers palate, select screen. You will notice that the chart throb is now the color that you selected in the Adobe 1998 Array chart! Print your new Chart Throb on a transparency.

Settings to use when printing your Chart Throb:

  • Set your printer to Printer Manages Color
  • Make sure to print without color management.
  • Print for Archival Matte paper at 2880 res
  • Flip image horizontal in order to print emulsion side down
  • Click Print

Section II

Through tests at UMBC we have found that a color setting of R-51 G-0 and B-43 works well with processes exposed on our UV table when negatives are printer on the Matte Black Epson 4800 printer. Test negatives are available preprinted with this color and the Chart Throb. These are located in the Alternative Processes room. Use the following process to make your curve for the process you are using.

  • Coat your paper your normal way and dry it. Make a test strip using a clear sheet of your transparency film. Process following your standard procedures. What you are looking for is the exposure that represents the minimum time it takes to make maximum density.
  • Coat another piece of paper, dry, and print the Chart Throb using the exposure time you found above. If you have the correct time, you will see that the chart has both bright whites and dark blacks. Look for a smooth grayscale.

How to analyze your Chart Throb:

  • Once the chart is dry, scan a preview of it using an Epson scanner.

  • Once the preview is complete, click on the box for Histogram Adjustment. Position the Input sliders so the black point and white point are touching the ends of the histogram. Check the Output slides they should be set to 0 and 255. Click Close. Click Scan.
  • Open scan in Photoshop.
  • Crop the chart to its edges.
  • Go to File/Scripts/ChartThrob.jsx
  • A dialog box will pop up. Click on “Analyze (your chart file name) Now”
  • After the computer calculates the curve, go to the layers palate and click on the box with the curve inside of it (#1 in the picture), then click on the drop down menu in the top right corner of the adjustments window (#2 in the picture). Select “Save Curves Preset”, and name the preset and save it on your desktop or jump drive.

Step By Set Guide To Printing Your Negatives

Preparing you image in Photoshop:

  • Open Image
  • Make preliminary Image adjustments
  • Crop/resize (360 ppi)
  • If image is color, convert to B&W
  • Set Black and White Levels
  • Flatten Image
  • Apply curve to image
  • Flatten Image
  • Invert your image
  • Convert back to RGB
  • Apply selected color to image R51, G0, B43
  • Change mode to screen
  • Flatten you image

Settings to use when printing your negatives:

  • Set media type to Archival Matte paper
  • Set print quality to Super Photo
  • Set color settings to OFF (No Color Management)
  • High Speed should be on
  • Flip horizontally if you haven’t done so already
  • Click Save
  • Click Print


Cyanotype

The earliest record of the cyanotype process are in research notes dated February 13, 1839 by Sir John Herschel, who formally announced it to the Royal Photographic Society of England three years later in June 1842.

Herschel’s only real application of cyanotypes was to make copies of his notes that he did not want to trust to the inaccuracies of hand transcription. He simply placed his notes over a sheet of cyanotype coated paper and exposed through the handwriting by sunlight, thus creating the first photocopy method.

The most famous early use of the process was for the book, Photographs of British Algae: Cyanotype Impressions, published in sections in the 1840’s by Anna Atkins. 411 original cyanotypes of seaweeds illustrated this book.

Cyanotype is a member of the family of iron salt processes that include the kallitype, the palladium print, and the platinotype which are considered by many to be the aristocracy of photographic printing processes. Relatively low material expense, ease of manipulation over a variety of surfaces, good permanence, and a long tonal range continue to make the cyanotype one of the most practical and attractive of most hand-applied emulsions.

Making a cyanotype is quite simple. The basic premise is that all ferric salts become light sensitive in the presence of organic substances. Most recipes call for the surface to be coated with a light-sensitive mixture of an iron compound ferric ammonium citrate and potassium ferricyanide. Exposure to UV light breaks the iron compound down by releasing carbon in the form of carbonic acid. When the exposed print is then immersed in water, this new compound, peroxide iron salt reacts with the potassium ferricyanide to form “Prussian blue”, a stable deep blue-colored compound.

Procedure: Cyanotype is slow you can work under low wattage tungsten light or under yellow bug lights.

If you intend to coat the cyanotype image again with another medium (e.g. gum print), and you want to keep both printings in good registration, pre-shrink the paper or cloth by soaking in hot water for 20 minutes and dry completely before applying any emulsion .

1. Apply solution onto desired surface. Because cyanotype solution does not have a vehicle such as gum arabic or gelatine, it should be thought of as a dye which must be allowed to soak into the fibers of the ground. The solution should be coated evenly, unless you desire a mottled image appearance. A sponge brush is the most efficient applicator for this purpose. Care must be taken not to re-coat an area which has already begun to dry, as the oxidizing process will be interrupted and the emulsion will begin to develop and neutralize itself, thus losing sensitivity to exposure. Place freshly coated paper in a drawer and allow it to set up for 5 minutes.

2. Hang up and allow to dry completely. Drying is somewhat tricky, especially in humidity. The emulsion should not be exposed until it is completely dry (a hair dryer is handy for speeding up the process, but be careful not to get the emulsion hot); if exposed when still damp it will not only develop while exposing (thus negating the image), but also the potassium ferricyanide in the emulsion will bleach out the silver if you are using film as your transparency. If allowed to sit too long after it is dry, the emulsion will lose sensitivity.

3. Once dry, expose under a transparency in a contact frame or under heavy enough glass to provide good contact. Exposure times are dependent upon the density of the transparency, and the degree of contrast and deepness of the blue color that you desire. Generally though, times range from 4 to 10 minutes in direct sunlight, 20 to 40 minutes in open shade, 6 to 12 minutes under our UV fluorescents. Exposures through paper negatives take 2 to 3 times as long.

4. Develop for 10 to 15 minutes (cloth may take longer) face down in running water, or until the base is clear and the yellow-green stain has completely disappeared; if not completely cleared, the cyanotype can still be affected and fogged by further exposure to UV light.

5. Hang up to dry. The blue color should deepen about one “zone” with drying. Be careful not to pick up stains from dirty clothespins. You can speed up the dry down processes by treating your prints in a bath of hydrogen peroxide. Mix 1 oz hydrogen peroxide to 32 oz of water. Wash another 10 minutes after this procedure.

Notes:

A. Occasionally the yellow stain will not clear; in that case, try a quick rinse in a 1:10 Dektol solution followed by a 5 to 10 minute wash. Well-diluted household ammonia also is a very controllable bleaching agent which can produce nicely colored results.

B. Cyanotypes on clothing need to be washed in a very gentle, non-alkaline/non-phosphate detergent, and preferably soft water; otherwise fading occurs quickly. Woolite and hand washing help greatly to prolong the life of cyanotype-cloths that get washed often.